OBSP Determination:
BENZO[A]PYRENE
METHOD: 4433 , TESTIDCODE: 34247GCM99

Analysis Date = 11/29/17 SpikeMix = ChemService 6541500: 100 µl & Abs 071317WWUF: 100 µl Pct Recovery = 75% Analysis Date = 09/27/17 SpikeMix = ChemService 6482500: 100 µl & ChemService 6507300: 100 µl Pct Recovery = 55% Analysis Date = 04/11/17 SpikeMix = Crescent 03FF070: 100 µl & Phenova B20160306: 100 µl Pct Recovery = 106% Analysis Date = 01/10/17 SpikeMix = ChemService 5016000: 100 µl & Crescent 03FF070: 100 µl Pct Recovery = 32% Analysis Date = 09/26/16 SpikeMix = Abs 061716WW: 100 µl & NSI 042916WW: 100 µl Pct Recovery = 53% Analysis Date = 02/24/16 SpikeMix = Spex Organics EN150529012: 80 µl & Crescent 04EE006: 80 µl Pct Recovery = 85% Analysis Date = 06/30/17 SpikeMix = Phenova B20160306: 80 µl & Crescent 03FF070: 80 µl Pct Recovery = 84% Analysis Date = 01/05/17 SpikeMix = Abs 061716WW: 80 µl & Crescent 03FF070: 80 µl Pct Recovery = 78% Analysis Date = 12/06/16 SpikeMix = Crescent 03FF070: 80 µl & Supelco LC20139V: 80 µl Pct Recovery = 72% Analysis Date = 08/10/16 SpikeMix = ChemService 5016000: 80 µl & Crescent 03FF070: 80 µl Pct Recovery = 78% Analysis Date = 08/15/17 SpikeMix = ChemService 5016000: 80 µl & NSI 042916WW: 80 µl Pct Recovery = 58% Analysis Date = 12/06/16 SpikeMix = Abs 061716WW: 80 µl & NSI 042916WW: 80 µl Pct Recovery = 68% Analysis Date = 12/06/16 SpikeMix = NSI 042916WW: 80 µl & Supelco LC20139V: 80 µl Pct Recovery = 53% Analysis Date = 03/14/18 SpikeMix = Abs 071417WWUF: 60 µl & ChemService 6507300: 60 µl Pct Recovery = 97% Analysis Date = 10/26/17 SpikeMix = ChemService 6507300: 60 µl & ChemService 6482500: 60 µl Pct Recovery = 79% Analysis Date = 09/27/17 SpikeMix = ChemService 6541500: 60 µl & ChemService 6507300: 60 µl Pct Recovery = 114% Analysis Date = 06/13/16 SpikeMix = ChemService 3982800: 40 µl & Crescent 04EE006: 40 µl Pct Recovery = 83% Analysis Date = 04/15/16 SpikeMix = ChemService 3982800: 40 µl & Abs 041615: 40 µl Pct Recovery = 75% Analysis Date = 05/25/17 SpikeMix = ChemService 5016000: 40 µl & Crescent 03FF070: 40 µl Pct Recovery = 66% Analysis Date = 10/06/16 SpikeMix = Crescent 03FF070: 40 µl & Supelco LC20139V: 40 µl Pct Recovery = 60% Analysis Date = 09/28/16 SpikeMix = Abs 061716WW: 40 µl & Crescent 03FF070: 40 µl Pct Recovery = 80% Analysis Date = 08/24/16 SpikeMix = Crescent 03FF070: 40 µl & Phenova B20160306: 40 µl Pct Recovery = 86% Analysis Date = 06/16/16 SpikeMix = Phenova B20160306: 40 µl & Crescent 03FF070: 40 µl Pct Recovery = 84% Analysis Date = 06/14/16 SpikeMix = ChemService 5016000: 40 µl & Crescent 03FF070: 40 µl Pct Recovery = 70% Analysis Date = 06/29/17 SpikeMix = Phenova B20160306: 40 µl & NSI 042916WW: 40 µl Pct Recovery = 69% Analysis Date = 04/12/17 SpikeMix = NSI 042916WW: 40 µl & Supelco LC20139V: 40 µl Pct Recovery = 94% Analysis Date = 12/07/16 SpikeMix = ChemService 5016000: 40 µl & NSI 042916WW: 40 µl Pct Recovery = 67% Analysis Date = 09/27/16 SpikeMix = NSI 042916WW: 40 µl & Phenova B20160306: 40 µl Pct Recovery = 69% Analysis Date = 08/03/16 SpikeMix = NSI 042916WW: 40 µl & Supelco LC20139V: 40 µl Pct Recovery = 75% Analysis Date = 10/26/17 SpikeMix = Abs 071417WWUF: 30 µl & Abs 071317WWUF: 30 µl Pct Recovery = 100% Analysis Date = 09/26/17 SpikeMix = ChemService 6482500: 30 µl & Abs 071317WWUF: 30 µl Pct Recovery = 105% Analysis Date = 04/16/16 SpikeMix = Crescent 04EE006: 20 µl & ERA 0406-15-02: 20 µl Pct Recovery = 67% Analysis Date = 02/24/16 SpikeMix = Abs 041615: 20 µl & Supelco LC13546: 20 µl Pct Recovery = 77% Analysis Date = 03/13/18 Pct Recovery = 94% Analysis Date = 03/10/18 Pct Recovery = 93% Analysis Date = 03/10/18 Pct Recovery = 93% Analysis Date = 03/06/18 Pct Recovery = 93% Analysis Date = 03/06/18 Pct Recovery = 93% Analysis Date = 03/02/18 Pct Recovery = 93% Analysis Date = 03/02/18 Pct Recovery = 93% Analysis Date = 02/27/18 Pct Recovery = 93% Analysis Date = 02/27/18 Pct Recovery = 93% Analysis Date = 02/23/18 Pct Recovery = 92% Analysis Date = 02/23/18 Pct Recovery = 92% Analysis Date = 02/19/18 Pct Recovery = 92% Analysis Date = 02/19/18 Pct Recovery = 92% Analysis Date = 02/15/18 Pct Recovery = 92% Analysis Date = 02/15/18 Pct Recovery = 92% Analysis Date = 02/12/18 Pct Recovery = 92% Analysis Date = 02/12/18 Pct Recovery = 92% Analysis Date = 02/08/18 Pct Recovery = 92% Analysis Date = 02/08/18 Pct Recovery = 92% Analysis Date = 02/04/18 Pct Recovery = 91% Analysis Date = 02/04/18 Pct Recovery = 91% Analysis Date = 01/31/18 Pct Recovery = 91% Analysis Date = 01/31/18 Pct Recovery = 91% Analysis Date = 01/28/18 Pct Recovery = 91% Analysis Date = 01/28/18 Pct Recovery = 91% Analysis Date = 01/24/18 Pct Recovery = 91% Analysis Date = 01/24/18 Pct Recovery = 91% Analysis Date = 01/20/18 Pct Recovery = 91% Analysis Date = 01/20/18 Pct Recovery = 91% Analysis Date = 01/16/18 Pct Recovery = 90% Analysis Date = 01/16/18 Pct Recovery = 90% Analysis Date = 01/13/18 Pct Recovery = 90% Analysis Date = 01/13/18 Pct Recovery = 90% Analysis Date = 01/09/18 Pct Recovery = 90% Analysis Date = 01/09/18 Pct Recovery = 90% Analysis Date = 01/05/18 Pct Recovery = 90% Analysis Date = 01/05/18 Pct Recovery = 90% Analysis Date = 01/01/18 Pct Recovery = 90% Analysis Date = 01/01/18 Pct Recovery = 90% Analysis Date = 12/29/17 Pct Recovery = 89% Analysis Date = 12/29/17 Pct Recovery = 89% Analysis Date = 12/25/17 Pct Recovery = 89% Analysis Date = 12/25/17 Pct Recovery = 89% Analysis Date = 12/21/17 Pct Recovery = 89% Analysis Date = 12/21/17 Pct Recovery = 89% Analysis Date = 12/17/17 Pct Recovery = 89% Analysis Date = 12/17/17 Pct Recovery = 89% Analysis Date = 12/14/17 Pct Recovery = 89% Analysis Date = 12/14/17 Pct Recovery = 89% Analysis Date = 12/10/17 Pct Recovery = 88% Analysis Date = 12/10/17 Pct Recovery = 88% Analysis Date = 12/06/17 Pct Recovery = 88% Analysis Date = 12/06/17 Pct Recovery = 88% Analysis Date = 12/02/17 Pct Recovery = 88% Analysis Date = 12/02/17 Pct Recovery = 88% Analysis Date = 11/29/17 Pct Recovery = 88% Analysis Date = 11/29/17 Pct Recovery = 88% Analysis Date = 11/25/17 Pct Recovery = 87% Analysis Date = 11/25/17 Pct Recovery = 87% Analysis Date = 11/21/17 Pct Recovery = 87% Analysis Date = 11/21/17 Pct Recovery = 87% Analysis Date = 11/17/17 Pct Recovery = 87% Analysis Date = 11/17/17 Pct Recovery = 87% Analysis Date = 11/14/17 Pct Recovery = 87% Analysis Date = 11/14/17 Pct Recovery = 87% Analysis Date = 11/10/17 Pct Recovery = 87% Analysis Date = 11/10/17 Pct Recovery = 87% Analysis Date = 11/06/17 Pct Recovery = 86% Analysis Date = 11/06/17 Pct Recovery = 86% Analysis Date = 11/02/17 Pct Recovery = 86% Analysis Date = 11/02/17 Pct Recovery = 86% Analysis Date = 10/30/17 Pct Recovery = 86% Analysis Date = 10/30/17 Pct Recovery = 86% Analysis Date = 10/26/17 Pct Recovery = 86% Analysis Date = 10/26/17 Pct Recovery = 86% Analysis Date = 10/22/17 Pct Recovery = 86% Analysis Date = 10/22/17 Pct Recovery = 86% Analysis Date = 10/18/17 Pct Recovery = 85% Analysis Date = 10/18/17 Pct Recovery = 85% Analysis Date = 10/15/17 Pct Recovery = 85% Analysis Date = 10/15/17 Pct Recovery = 85% Analysis Date = 10/11/17 Pct Recovery = 85% Analysis Date = 10/11/17 Pct Recovery = 85% Analysis Date = 10/07/17 Pct Recovery = 85% Analysis Date = 10/07/17 Pct Recovery = 85% Analysis Date = 10/03/17 Pct Recovery = 85% Analysis Date = 10/03/17 Pct Recovery = 85% Analysis Date = 09/30/17 Pct Recovery = 85% Analysis Date = 09/30/17 Pct Recovery = 85% Analysis Date = 09/26/17 Pct Recovery = 84% Analysis Date = 09/26/17 Pct Recovery = 84% Analysis Date = 09/22/17 Pct Recovery = 84% Analysis Date = 09/22/17 Pct Recovery = 84% Analysis Date = 09/18/17 Pct Recovery = 84% Analysis Date = 09/18/17 Pct Recovery = 84% Analysis Date = 09/15/17 Pct Recovery = 84% Analysis Date = 09/15/17 Pct Recovery = 84% Analysis Date = 09/11/17 Pct Recovery = 84% Analysis Date = 09/11/17 Pct Recovery = 84% Analysis Date = 09/07/17 Pct Recovery = 84% Analysis Date = 09/07/17 Pct Recovery = 84% Analysis Date = 09/04/17 Pct Recovery = 83% Analysis Date = 09/04/17 Pct Recovery = 83% Analysis Date = 08/31/17 Pct Recovery = 83% Analysis Date = 08/31/17 Pct Recovery = 83% Analysis Date = 08/27/17 Pct Recovery = 83% Analysis Date = 08/27/17 Pct Recovery = 83% Analysis Date = 08/23/17 Pct Recovery = 83% Analysis Date = 08/23/17 Pct Recovery = 83% Analysis Date = 08/20/17 Pct Recovery = 83% Analysis Date = 08/20/17 Pct Recovery = 83% Analysis Date = 08/16/17 Pct Recovery = 83% Analysis Date = 08/16/17 Pct Recovery = 83% Analysis Date = 08/12/17 Pct Recovery = 82% Analysis Date = 08/12/17 Pct Recovery = 82% Analysis Date = 08/08/17 Pct Recovery = 82% Analysis Date = 08/08/17 Pct Recovery = 82% Analysis Date = 08/05/17 Pct Recovery = 82% Analysis Date = 08/05/17 Pct Recovery = 82% Analysis Date = 08/01/17 Pct Recovery = 82% Analysis Date = 08/01/17 Pct Recovery = 82% Analysis Date = 07/28/17 Pct Recovery = 82% Analysis Date = 07/28/17 Pct Recovery = 82% Analysis Date = 07/24/17 Pct Recovery = 82% Analysis Date = 07/24/17 Pct Recovery = 82% Analysis Date = 07/21/17 Pct Recovery = 81% Analysis Date = 07/21/17 Pct Recovery = 81% Analysis Date = 07/17/17 Pct Recovery = 81% Analysis Date = 07/17/17 Pct Recovery = 81% Analysis Date = 07/13/17 Pct Recovery = 81% Analysis Date = 07/13/17 Pct Recovery = 81% Analysis Date = 07/09/17 Pct Recovery = 81% Analysis Date = 07/09/17 Pct Recovery = 81% Analysis Date = 07/06/17 Pct Recovery = 81% Analysis Date = 07/06/17 Pct Recovery = 81% Analysis Date = 07/02/17 Pct Recovery = 81% Analysis Date = 07/02/17 Pct Recovery = 81% Analysis Date = 06/28/17 Pct Recovery = 80% Analysis Date = 06/28/17 Pct Recovery = 80% Analysis Date = 06/24/17 Pct Recovery = 80% Analysis Date = 06/24/17 Pct Recovery = 80% Analysis Date = 06/21/17 Pct Recovery = 80% Analysis Date = 06/21/17 Pct Recovery = 80% Analysis Date = 06/17/17 Pct Recovery = 80% Analysis Date = 06/17/17 Pct Recovery = 80% Analysis Date = 06/13/17 Pct Recovery = 79% Analysis Date = 06/13/17 Pct Recovery = 79% Analysis Date = 06/09/17 Pct Recovery = 79% Analysis Date = 06/09/17 Pct Recovery = 79% Analysis Date = 06/06/17 Pct Recovery = 79% Analysis Date = 06/06/17 Pct Recovery = 79% Analysis Date = 06/02/17 Pct Recovery = 79% Analysis Date = 06/02/17 Pct Recovery = 79% Analysis Date = 05/29/17 Pct Recovery = 78% Analysis Date = 05/29/17 Pct Recovery = 78% Analysis Date = 05/25/17 Pct Recovery = 78% Analysis Date = 05/25/17 Pct Recovery = 78% Analysis Date = 05/22/17 Pct Recovery = 78% Analysis Date = 05/22/17 Pct Recovery = 78% Analysis Date = 05/18/17 Pct Recovery = 78% Analysis Date = 05/18/17 Pct Recovery = 78% Analysis Date = 05/14/17 Pct Recovery = 77% Analysis Date = 05/14/17 Pct Recovery = 77% Analysis Date = 05/10/17 Pct Recovery = 77% Analysis Date = 05/10/17 Pct Recovery = 77% Analysis Date = 05/07/17 Pct Recovery = 77% Analysis Date = 05/07/17 Pct Recovery = 77% Analysis Date = 05/03/17 Pct Recovery = 77% Analysis Date = 05/03/17 Pct Recovery = 77% Analysis Date = 04/29/17 Pct Recovery = 76% Analysis Date = 04/29/17 Pct Recovery = 76% Analysis Date = 04/25/17 Pct Recovery = 76% Analysis Date = 04/25/17 Pct Recovery = 76% Analysis Date = 04/22/17 Pct Recovery = 76% Analysis Date = 04/22/17 Pct Recovery = 76% Analysis Date = 04/18/17 Pct Recovery = 75% Analysis Date = 04/18/17 Pct Recovery = 75% Analysis Date = 04/14/17 Pct Recovery = 75% Analysis Date = 04/14/17 Pct Recovery = 75% Analysis Date = 04/10/17 Pct Recovery = 75% Analysis Date = 04/10/17 Pct Recovery = 75% Analysis Date = 04/07/17 Pct Recovery = 75% Analysis Date = 04/07/17 Pct Recovery = 75% Analysis Date = 04/03/17 Pct Recovery = 75% Analysis Date = 04/03/17 Pct Recovery = 75% Analysis Date = 03/30/17 Pct Recovery = 74% Analysis Date = 03/30/17 Pct Recovery = 74% Analysis Date = 03/26/17 Pct Recovery = 74% Analysis Date = 03/26/17 Pct Recovery = 74% Analysis Date = 03/23/17 Pct Recovery = 74% Analysis Date = 03/23/17 Pct Recovery = 74% Analysis Date = 03/19/17 Pct Recovery = 74% Analysis Date = 03/19/17 Pct Recovery = 74% Analysis Date = 03/15/17 Pct Recovery = 74% Analysis Date = 03/15/17 Pct Recovery = 74% Analysis Date = 03/11/17 Pct Recovery = 74% Analysis Date = 03/11/17 Pct Recovery = 74% Analysis Date = 03/08/17 Pct Recovery = 73% Analysis Date = 03/08/17 Pct Recovery = 73% Analysis Date = 03/04/17 Pct Recovery = 73% Analysis Date = 03/04/17 Pct Recovery = 73% Analysis Date = 02/28/17 Pct Recovery = 73% Analysis Date = 02/28/17 Pct Recovery = 73% Analysis Date = 02/25/17 Pct Recovery = 73% Analysis Date = 02/25/17 Pct Recovery = 73% Analysis Date = 02/21/17 Pct Recovery = 73% Analysis Date = 02/21/17 Pct Recovery = 73% Analysis Date = 02/17/17 Pct Recovery = 73% Analysis Date = 02/17/17 Pct Recovery = 73% Analysis Date = 02/13/17 Pct Recovery = 72% Analysis Date = 02/13/17 Pct Recovery = 72% Analysis Date = 02/10/17 Pct Recovery = 72% Analysis Date = 02/10/17 Pct Recovery = 72% Analysis Date = 02/06/17 Pct Recovery = 72% Analysis Date = 02/06/17 Pct Recovery = 72% Analysis Date = 02/02/17 Pct Recovery = 72% Analysis Date = 02/02/17 Pct Recovery = 72% Analysis Date = 01/29/17 Pct Recovery = 72% Analysis Date = 01/29/17 Pct Recovery = 72% Analysis Date = 01/26/17 Pct Recovery = 72% Analysis Date = 01/26/17 Pct Recovery = 72% Analysis Date = 01/22/17 Pct Recovery = 72% Analysis Date = 01/22/17 Pct Recovery = 72% Analysis Date = 01/18/17 Pct Recovery = 71% Analysis Date = 01/18/17 Pct Recovery = 71% Analysis Date = 01/14/17 Pct Recovery = 71% Analysis Date = 01/14/17 Pct Recovery = 71% Analysis Date = 01/11/17 Pct Recovery = 71% Analysis Date = 01/11/17 Pct Recovery = 71% Analysis Date = 01/07/17 Pct Recovery = 71% Analysis Date = 01/07/17 Pct Recovery = 71% Analysis Date = 01/03/17 Pct Recovery = 71% Analysis Date = 01/03/17 Pct Recovery = 71% Analysis Date = 12/30/16 Pct Recovery = 70% Analysis Date = 12/30/16 Pct Recovery = 70% Analysis Date = 12/27/16 Pct Recovery = 69% Analysis Date = 12/27/16 Pct Recovery = 69% Analysis Date = 12/23/16 Pct Recovery = 69% Analysis Date = 12/23/16 Pct Recovery = 69% Analysis Date = 12/19/16 Pct Recovery = 68% Analysis Date = 12/19/16 Pct Recovery = 68% Analysis Date = 12/15/16 Pct Recovery = 68% Analysis Date = 12/15/16 Pct Recovery = 68% Analysis Date = 12/12/16 Pct Recovery = 67% Analysis Date = 12/12/16 Pct Recovery = 67% Analysis Date = 12/08/16 Pct Recovery = 67% Analysis Date = 12/08/16 Pct Recovery = 67% Analysis Date = 12/04/16 Pct Recovery = 66% Analysis Date = 12/04/16 Pct Recovery = 66% Analysis Date = 11/30/16 Pct Recovery = 67% Analysis Date = 11/30/16 Pct Recovery = 67% Analysis Date = 11/27/16 Pct Recovery = 67% Analysis Date = 11/27/16 Pct Recovery = 67% Analysis Date = 11/23/16 Pct Recovery = 67% Analysis Date = 11/23/16 Pct Recovery = 67% Analysis Date = 11/19/16 Pct Recovery = 67% Analysis Date = 11/19/16 Pct Recovery = 67% Analysis Date = 11/15/16 Pct Recovery = 67% Analysis Date = 11/15/16 Pct Recovery = 67% Analysis Date = 11/12/16 Pct Recovery = 67% Analysis Date = 11/12/16 Pct Recovery = 67% Analysis Date = 11/08/16 Pct Recovery = 68% Analysis Date = 11/08/16 Pct Recovery = 68% Analysis Date = 11/04/16 Pct Recovery = 68% Analysis Date = 11/04/16 Pct Recovery = 68% Analysis Date = 10/31/16 Pct Recovery = 68% Analysis Date = 10/31/16 Pct Recovery = 68% Analysis Date = 10/28/16 Pct Recovery = 68% Analysis Date = 10/28/16 Pct Recovery = 68% Analysis Date = 10/24/16 Pct Recovery = 68% Analysis Date = 10/24/16 Pct Recovery = 68% Analysis Date = 10/20/16 Pct Recovery = 69% Analysis Date = 10/20/16 Pct Recovery = 69% Analysis Date = 10/16/16 Pct Recovery = 69% Analysis Date = 10/16/16 Pct Recovery = 69% Analysis Date = 10/13/16 Pct Recovery = 69% Analysis Date = 10/13/16 Pct Recovery = 69% Analysis Date = 10/09/16 Pct Recovery = 69% Analysis Date = 10/09/16 Pct Recovery = 69% Analysis Date = 10/05/16 Pct Recovery = 69% Analysis Date = 10/05/16 Pct Recovery = 69% Analysis Date = 10/01/16 Pct Recovery = 69% Analysis Date = 10/01/16 Pct Recovery = 69% Analysis Date = 09/28/16 Pct Recovery = 70% Analysis Date = 09/28/16 Pct Recovery = 70% Analysis Date = 09/24/16 Pct Recovery = 70% Analysis Date = 09/24/16 Pct Recovery = 70% Analysis Date = 09/20/16 Pct Recovery = 70% Analysis Date = 09/20/16 Pct Recovery = 70% Analysis Date = 09/16/16 Pct Recovery = 70% Analysis Date = 09/16/16 Pct Recovery = 70% Analysis Date = 09/13/16 Pct Recovery = 71% Analysis Date = 09/13/16 Pct Recovery = 71% Analysis Date = 09/09/16 Pct Recovery = 71% Analysis Date = 09/09/16 Pct Recovery = 71% Analysis Date = 09/05/16 Pct Recovery = 71% Analysis Date = 09/05/16 Pct Recovery = 71% Analysis Date = 09/01/16 Pct Recovery = 72% Analysis Date = 09/01/16 Pct Recovery = 72% Analysis Date = 08/29/16 Pct Recovery = 72% Analysis Date = 08/29/16 Pct Recovery = 72% Analysis Date = 08/25/16 Pct Recovery = 72% Analysis Date = 08/25/16 Pct Recovery = 72% Analysis Date = 08/21/16 Pct Recovery = 73% Analysis Date = 08/21/16 Pct Recovery = 73% Analysis Date = 08/18/16 Pct Recovery = 73% Analysis Date = 08/18/16 Pct Recovery = 73% Analysis Date = 08/14/16 Pct Recovery = 73% Analysis Date = 08/14/16 Pct Recovery = 73% Analysis Date = 08/10/16 Pct Recovery = 74% Analysis Date = 08/10/16 Pct Recovery = 74% Analysis Date = 08/06/16 Pct Recovery = 74% Analysis Date = 08/06/16 Pct Recovery = 74% Analysis Date = 08/03/16 Pct Recovery = 74% Analysis Date = 08/03/16 Pct Recovery = 74% Analysis Date = 07/30/16 Pct Recovery = 74% Analysis Date = 07/30/16 Pct Recovery = 74% Analysis Date = 07/26/16 Pct Recovery = 74% Analysis Date = 07/26/16 Pct Recovery = 74% Analysis Date = 07/22/16 Pct Recovery = 74% Analysis Date = 07/22/16 Pct Recovery = 74% Analysis Date = 07/19/16 Pct Recovery = 74% Analysis Date = 07/19/16 Pct Recovery = 74% Analysis Date = 07/15/16 Pct Recovery = 74% Analysis Date = 07/15/16 Pct Recovery = 74% Analysis Date = 07/11/16 Pct Recovery = 75% Analysis Date = 07/11/16 Pct Recovery = 75% Analysis Date = 07/07/16 Pct Recovery = 75% Analysis Date = 07/07/16 Pct Recovery = 75% Analysis Date = 07/04/16 Pct Recovery = 75% Analysis Date = 07/04/16 Pct Recovery = 75% Analysis Date = 06/30/16 Pct Recovery = 75% Analysis Date = 06/30/16 Pct Recovery = 75% Analysis Date = 06/26/16 Pct Recovery = 75% Analysis Date = 06/26/16 Pct Recovery = 75% Analysis Date = 06/22/16 Pct Recovery = 75% Analysis Date = 06/22/16 Pct Recovery = 75% Analysis Date = 06/19/16 Pct Recovery = 75% Analysis Date = 06/19/16 Pct Recovery = 75% Analysis Date = 06/15/16 Pct Recovery = 76% Analysis Date = 06/15/16 Pct Recovery = 76% Analysis Date = 06/11/16 Pct Recovery = 76% Analysis Date = 06/11/16 Pct Recovery = 76% Analysis Date = 06/07/16 Pct Recovery = 76% Analysis Date = 06/07/16 Pct Recovery = 76% Analysis Date = 06/04/16 Pct Recovery = 76% Analysis Date = 06/04/16 Pct Recovery = 76% Analysis Date = 05/31/16 Pct Recovery = 76% Analysis Date = 05/31/16 Pct Recovery = 76% Analysis Date = 05/27/16 Pct Recovery = 76% Analysis Date = 05/27/16 Pct Recovery = 76% Analysis Date = 05/23/16 Pct Recovery = 76% Analysis Date = 05/23/16 Pct Recovery = 76% Analysis Date = 05/20/16 Pct Recovery = 76% Analysis Date = 05/20/16 Pct Recovery = 76% Analysis Date = 05/16/16 Pct Recovery = 77% Analysis Date = 05/16/16 Pct Recovery = 77% Analysis Date = 05/12/16 Pct Recovery = 77% Analysis Date = 05/12/16 Pct Recovery = 77% Analysis Date = 05/08/16 Pct Recovery = 77% Analysis Date = 05/08/16 Pct Recovery = 77% Analysis Date = 05/05/16 Pct Recovery = 77% Analysis Date = 05/05/16 Pct Recovery = 77% Analysis Date = 05/01/16 Pct Recovery = 77% Analysis Date = 05/01/16 Pct Recovery = 77% Analysis Date = 04/27/16 Pct Recovery = 77% Analysis Date = 04/27/16 Pct Recovery = 77% Analysis Date = 04/23/16 Pct Recovery = 77% Analysis Date = 04/23/16 Pct Recovery = 77% Analysis Date = 04/20/16 Pct Recovery = 77% Analysis Date = 04/20/16 Pct Recovery = 77% Analysis Date = 04/16/16 Pct Recovery = 78% Analysis Date = 04/16/16 Pct Recovery = 78% Analysis Date = 04/12/16 Pct Recovery = 78% Analysis Date = 04/12/16 Pct Recovery = 78% Analysis Date = 04/08/16 Pct Recovery = 78% Analysis Date = 04/08/16 Pct Recovery = 78% Analysis Date = 04/05/16 Pct Recovery = 78% Analysis Date = 04/05/16 Pct Recovery = 78% Analysis Date = 04/01/16 Pct Recovery = 78% Analysis Date = 04/01/16 Pct Recovery = 78% Analysis Date = 03/28/16 Pct Recovery = 78% Analysis Date = 03/28/16 Pct Recovery = 78% Analysis Date = 03/24/16 Pct Recovery = 78% Analysis Date = 03/24/16 Pct Recovery = 78% Analysis Date = 03/21/16 Pct Recovery = 78% Analysis Date = 03/21/16 Pct Recovery = 78% Analysis Date = 03/17/16 Pct Recovery = 78% Analysis Date = 03/17/16 Pct Recovery = 78% Analysis Date = 03/13/16 Pct Recovery = 78% Analysis Date = 03/13/16 Pct Recovery = 78% Analysis Date = 03/09/16 Pct Recovery = 79% Analysis Date = 03/09/16 Pct Recovery = 79% Analysis Date = 03/06/16 Pct Recovery = 79% Analysis Date = 03/06/16 Pct Recovery = 79% Analysis Date = 03/02/16 Pct Recovery = 79% Analysis Date = 03/02/16 Pct Recovery = 79% Analysis Date = 02/27/16 Pct Recovery = 79% Analysis Date = 02/27/16 Pct Recovery = 79% Analysis Date = 02/24/16 Pct Recovery = 79% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
BENZO[A]PYRENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 33 76% 17% 75% 13%
Total 33 76% 17% 75% 13%

Sample Statistics
BENZO[A]PYRENE

Characteristic N % % Basis
Plotted 33 92% Spiked
Estimated Values 3 8% Spiked
Deleted Values 2 4% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 37 .  
False Negatives 3 8% 3 out of 36
Not Spiked 18 .  
False Positives 0 0% 0 out of 17